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1 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product name: Trade Names: Graphene oxide powder Graphenea Graphene Oxide Powder. EC # Relevant identified uses of the substance or mixture and uses advised against Identified uses: Research use Details of the supplier of the safety data sheet Graphenea Inc. 1 Broadway, Cambridge, MA USA for SDS: Phone: (+1) Emergency telephone number (+1) SECTION 2: Hazards identification 2.1. Classification of the substance or mixture Not classified as a hazardous substance according to GHS (rev. 5). Please notice that substance properties used for the hazard assessment come from graphite (bulk substance). The properties of the nanoform are under evaluation and to some extent not known Label elements No label required 2.3. Other hazards Physical Hazards: Care should be taken to avoid accumulations of graphene oxide dusts or powders in places where these accumulations could cause shorting of electrical switches, circuits or components. Graphenea - Graphene Oxide Powder Page 1 / 9

2 SECTION 3: Composition/information on ingredients 3.1. Substances Substance name Description Graphene oxide Graphene oxide is a thin layer of oxidized carbon; it is a single, tightly packed layer of carbon atoms that are bonded together in a hexagonal honeycomb lattice. EC SECTION 4: First aid measures 4.1. Description of first aid measures Inhalation Ingestion Skin contact Eye contact In case of discomfort provide fresh air, warmth and rest, preferably in a comfortable upright sitting position. Rinse nose and mouth with water. Get medical attention if any discomfort continues. If breathing stops, provide artificial respiration. NEVER MAKE AN UNCONSCIOUS PERSON VOMIT OR DRINK FLUIDS! Rinse nose, mouth and throat with water, and then drink plenty of water. Get medical attention. Wash skin with soap and water. Continue to rinse for at least 15 minutes. Get medical attention if irritation appears after washing. Do not rub eye. Immediately flush with plenty of water for up to minutes. Remove any contact lenses after 5 minutes, maintain open eyes wide apart. Get medical attention promptly if symptoms occur after washing Most important symptoms and effects, both acute and delayed Inhalation Ingestion Skin contact Eye contact Delayed effects It may cause irritation to respiratory tract/inhalation No effects recorded It may cause skin irritation. It may cause eye irritation. No delayed effects known Indication of any immediate medical attention and special treatment needed Treat symptomatically. Contact a medical centre immediately in case of ingestion or inhalation of a large amount of product. Specific treatment: No specific treatment. Graphenea - Graphene Oxide Powder Page 2 / 9

3 SECTION 5: Firefighting measures 5.1. Extinguishing media Suitable extinguishing media: The substance is not combustible, use extinguishing measures that are appropriate to local circumstances and the surrounding environment Special hazards arising from the substance or mixture In the event of combustion or thermal decomposition, this material may release carbon monoxide (CO) or carbon dioxide (CO2) or other toxic gases. IN CASE OF THERMAL TREATMENT PLEASE DO IT CAREFULLY AT SLOW HEATING RAMPS. ENERGY REALISE AT TEMPERATURES AROUND 180ºC. At temperatures over 180ºC, this material may react with potassium, sodium, rubidium, or cesium to create intercalation compounds that may ignite and may react explosively with water Advice for firefighters In general, graphene oxide is difficult to combust. Normal care should be taken to avoid dust explosion risk caused by high concentrations of dust or finely suspended airborne particles (although graphite dust is not normally considered to have an explosive hazard). Use respiratory protective equipment. SECTION 6: Accidental release measures 6.1. Personal precautions, protective equipment and emergency procedures Emergency responders should wear suitable protective equipment to prevent inhalation or skin contact. In case of spills, beware of slippery floors and surfaces Environmental precautions Do not allow to enter drains, sewers or watercourses. The product should not be dumped in nature but collected and delivered according to local regulations Methods and material for containment and cleaning up Spilled or released material should be collected mechanically and disposed of in suitable containers. Prevent dust generation Reference to other sections For personal protection, see section 8. For waste disposal, see section 13. SECTION 7: Handling and storage 7.1. Precautions for safe handling Avoid contact with skin and eyes. Wear personal protective equipment to prevent skin and eye contact. Do not wear contact lenses when using this product. Prevent dust generation. Avoid dust inhalation using local ventilation or appropriate filters. Graphenea - Graphene Oxide Powder Page 3 / 9

4 7.2. Conditions for safe storage, including any incompatibilities This material should be stored in labelled closed containers away from sources of ignition or heat. Care should be taken to avoid creating accumulations or concentrations of dust Specific end use(s) Research use. SECTION 8: Exposure controls/personal protection 8.1. Control parameters Substance: Graphite (CAS ) Limit value - Eight hours Limit value - Short term ppm mg/m³ ppm mg/m³ Australia 3 (1)(2)(3)(4) Belgium 2 Canada - Ontario 2 (1) Canada - Québec 2 Denmark 2,5 respirable aerosol 5 respirable aerosol Finland 2 France Germany (DFG) Ireland 10 (1) 2 respirable aerosol 4 inhalable aerosol 1,5 respirable aerosol 4 (2) Latvia 2 (1 New Zealand 3 (1)(2) People's Republic of China Singapore 4 (1) 2 (2) South Korea 2 (1)(2) Spain Sweden Switzerland USA - NIOSH 2,5 (1) USA - OSHA United Kingdom 2 respirable aerosol 2 inhalable aerosol 5 inhalable aerosol 5 inhalable aerosol 2,5 respirable aerosol 15 total dust 5 respirable dust 10 inhalable aerosol 4 respirable aerosol Graphenea - Graphene Oxide Powder Page 4 / 9

5 Remarks Australia Canada - Ontario Ireland Latvia New Zealand People's Republic of China South Korea USA - NIOSH (1) all forms except fibres (2) respirable aerosol (3) natural and synthetic (4) containing no asbestos and<="" td=""> (1) Respirable aerosol (1) Inhalable fraction (2) Respirable fraction (1) natural and industrial diamond, graphite (1) Respirable dust containing <1 % free silica (2) all form except graphite fibres (1) Inhalable fraction (2) Respirable fraction (1) Natural & synthetic except graphite fibers (2) Respirable fraction (1) natural graphite 8.2. Exposure controls Protective equipment P3 Engineering measures Provide adequate ventilation. Observe Occupational Exposure Limits and minimise the risk of inhalation of dust. Local exhaust ventilation should be employed if dust is generated when handling. Provide eyewash station. Personal Protective Equipment Respiratory equipment Hand protection Eye protection Body protection Respiratory protection must be used if the general level exceeds the recommended occupational exposure limit. A respiratory protection program that meets applicable OHSA (USA) or CEN (UE) requirements should be maintained in the workplace. When manipulating the powder out of a fume hood P3 dust mask should be used. Wear protective gloves. Wear approved safety goggles. Use face shield in case of splash risk. Wear full body industrial type work clothing. Environmental exposure controls All ventilation systems should be filtered before discharge to atmosphere. Avoid releasing to the environment. Avoid uncontrolled releases. Inform competent authorities in case large spillage into water courses. SECTION 9: Physical and chemical properties 9.1. Information on basic physical and chemical properties Appearance Colour Odour Initial boiling point and boiling range (ºC) Powder Brown Odourless Graphenea - Graphene Oxide Powder Page 5 / 9

6 Melting point (ºC) Vapour density (air=1) Vapour pressure Evaporation rate ph-value, Conc. Solution Not applicable Viscosity 40ºC Bulk density g/cm3 Solubility Value Negligible. Decomposition temperature ( C) - Flash point ( C) Auto Ignition Temperature ( C) Not applicable Oxidising properties Not applicable (the substance is incapable of reacting exothermically with combustible materials on the basis of chemical structure)) Other information SECTION 10: Stability and reactivity Reactivity There are no known reactivity hazards associated with this product Chemical stability Stable under normal temperature conditions Possibility of hazardous reactions At temperatures over 180ºC, this material may release energy and may react with potassium, sodium, rubidium, or cesium to create intercalation compounds that may ignite and may react explosively with water Conditions to avoid Not known Incompatible materials Avoid contact with strong oxidizing agents, fluorine, or chlorine trifluoride Hazardous decomposition products Under fire conditions, this material may release carbon monoxide (CO) or carbon dioxide (CO2) or other toxic gases. Graphenea - Graphene Oxide Powder Page 6 / 9

7 SECTION 11: Toxicological information Information on toxicological effects Absorption, distribution, metabolism Absorption Distribution Potential for accumulation Toxicologically significant metabolite Acute toxicity Rat LD50 oral Rat LD50 dermal Rat LC50 inhalation Skin irritation Eye irritation Skin sensitization Genotoxicity OECD 476: In vitro mammalian cell gene mutation test Negative OECD 487: In vitro mammalian cell micronucleus test Negative Long term toxicity and Carcinogenicity Reproductive toxicity SECTION 12: Ecological information Toxicity Persistence and degradability Bioaccumulative potential Mobility in soil Graphenea - Graphene Oxide Powder Page 7 / 9

8 12.5. Other adverse effects SECTION 13: Disposal considerations Waste treatment methods General information When handling waste, consideration should be made to the safety precautions applying to handling of the product. Waste should not be disposed of by release to sewers. Uncleaned packagings: Disposal must be made according to official regulations. SECTION 14: Transport information UN number Not classified as a dangerous good for transport under DOT, IMDG, ADR, RID, or ICAO/IATA UN proper shipping name Transport hazard class(es) Packing group Environmental hazards Special precautions for user Transport in bulk according to Annex II of Marpol and the IBC Code Graphenea - Graphene Oxide Powder Page 8 / 9

9 SECTION 15: Regulatory information Safety, health and environmental regulations/legislation specific for the substance or mixture SARA 302 Components: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302. SARA 313 Components: This material does not contain any chemical components with known CAS numbers that exceed the threshold (De Minimis) reporting levels established by SARA Title III, Section 313. SARA 311/312 Hazards: No SARA Hazards Massachusetts Right To Know Components: No components are subject to the Massachusetts Right to Know Act. New Jersey Right To Know Components: CAS-No. Water Pennsylvania Right To Know Components: CAS-No. Water California Prop. 65 Components: This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm. TSCA: not listed. R&D only. SECTION 16: Other information Advice on any training appropriate for workers Revision Date 05 March 2020 Substituted version 7.0 To ensure protection of human health and environment, workers must be provided with proper training about how to handle and store chemicals used at work. This information is based on our present state of knowledge and our research into available scientific literature as well as information obtained from our vendors. Graphenea S.A. makes no responsibility regarding the accuracy of the scientific literature or any thirdparty information and, therefore, cannot guarantee any specific material properties. Use of this information shall not establish a legally binding relationship. The information provided in this SDS must be considered as a starting point for a comprehensive program of health and safety in your company. If further data on the product is required to perform your risk assessment, contact us and we will try to assist as much as possible. Graphenea - Graphene Oxide Powder Page 9 / 9

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